Detail předmětu

Instrumental and structural analysis

FCH-MA_ISAAk. rok: 2021/2022

The students will be acquainted with theoretical fundamentals and application of methods of chemical, physical and structural analysis. The course also includes advanced separation and electromigration techniques, organic Mass Spectrometry with emphasis on tandem techniques, Infrared and Raman Spectroscopy, Thermogravimetry, Differential Thermal Analysis, Differential Scanning Calorimetry, X-Ray Fluorescence, X-Ray Diffraction, Auger Electron Spectroscopy, Nuclear Magnetic Resonance and Electron Microscopy. The overview is completed with inorganic analysis techniques, such as Atomic Absorption Spectrometry, Emission and Fluorescence Spectrometry together with Inductively Coupled Plasma Mass Spectrometry and Inductively Coupled Plasma Optical Emission Spectrometry.

Jazyk výuky

angličtina

Počet kreditů

4

Nabízen zahraničním studentům

Pouze domovské fakulty

Způsob a kritéria hodnocení

Written examination including all topics discussed. If more than 50% are obtained, an oral exam follows. The knowledge of principles of analytical methods including their particularities, and ability of creative solution of analytical problems are evaluated. Final evaluation corresponds to ECTS system.

Osnovy výuky

The students will be acquainted with theoretical fundamentals and application of methods of chemical, physical and structural analysis. The course also includes advanced separation and electromigration techniques, organic Mass Spectrometry with emphasis on tandem techniques, Infrared and Raman Spectroscopy, Thermogravimetry, Differential Thermal Analysis, Differential Scanning Calorimetry, X-Ray Fluorescence, X-Ray Diffraction, Auger Electron Spectroscopy, Nuclear Magnetic Resonance and Electron Microscopy. The overview is completed with inorganic analysis techniques, such as Atomic Absorption Spectrometry, Emission and Fluorescence Spectrometry together with Inductively Coupled Plasma Mass Spectrometry and Inductively Coupled Plasma Optical Emission Spectrometry.

1. Advanced separation techniques
2. Electromigration methods
3. Organic Mass Spectrometry
4. Infrared Spectroscopy, Raman Spectroscopy
5. Atomic Absorption Spectrometry
6. Atomic Emission Spectrometry (AES, AFS), Inductively Coupled Plasma spectrometry
7. Inductively Coupled Plasma Mass Spectrometry, Inductively Coupled Plasma Optical Emission Spectrometry
8. Thermal Analysis – Thermogravimetry, simultaneous methods
9. Thermal Analysis – Differential Thermal Analysis, Differential Scanning Calorimetry
10. X-Ray Fluorescence, Auger Electron Spectroscopy
11. Electron Microscopy
12. X-Ray Diffraction
13. Nuclear Magnetic Resonance

Učební cíle

The students will be informed about selected methods used for structural analysis, and advanced analytical technique designed to organic and inorganic chemical analysis. The fundamental characteristic of methods and their applications in solving specific analytical problems will be discussed.

Vymezení kontrolované výuky a způsob jejího provádění a formy nahrazování zameškané výuky

Attendance at the lecture is not required, but recommended.

Základní literatura

Crouch S. a Skoog D., Principles of Instrumental Analysis, Cengage Learning, Inc., 2017. (EN)
Kellner R., Mermet J. M., Otto M., Widmer H. M.: Analytical Chemistry. Willey-VCH, Weinheim 1998. (EN)
Skoog D. A., West D. M., Holler F. J., Crouch S. R.: Fundamentals of Analytical Chemistry, Cengage Learning, Inc., 2014. (EN)

eLearning

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