Detail publikace

THE DESIGN OF SAMPLE HOLDER FOR XRD MEASUREMENTS IN INERT ATMOSPHERE WITH DISPLACEMENT ERROR CORRECTION

KLVAČ, O.

Originální název

THE DESIGN OF SAMPLE HOLDER FOR XRD MEASUREMENTS IN INERT ATMOSPHERE WITH DISPLACEMENT ERROR CORRECTION

Typ

článek ve sborníku ve WoS nebo Scopus

Jazyk

angličtina

Originální abstrakt

This article describes a designed of a holder for post-mortem XRD measurements of Li-ion, Na-ion and Li-S electrodes, which need to be performed in the inert atmosphere. The first part describes the measurement method and problems arising during the measurements of the samples. Subsequently, the design and construction of a new cell with hermetic insulation and sample displacement error correction possible during the operation of the diffractometer is described. Finally, the inert gas attenuation within the cell is theoretically calculated. The calculation is verified by practical measurements, and alternatives are proposed to improve the signal-to-noise ratio.

Klíčová slova

XRD, ex-situ, post-mortem, sample displacement, attenuation, SNR

Autoři

KLVAČ, O.

Vydáno

23. 4. 2020

ISBN

978-80-214-5868-0

Kniha

Proceedings of the 26th Conference STUDENT EEICT 2020 Selected Papers

Edice

1

Číslo edice

25

Strany od

103

Strany do

107

Strany počet

5

BibTex

@inproceedings{BUT166188,
  author="Ondřej {Klvač}",
  title="THE DESIGN OF SAMPLE HOLDER FOR XRD MEASUREMENTS IN INERT ATMOSPHERE WITH DISPLACEMENT ERROR CORRECTION",
  booktitle="Proceedings of the 26th Conference STUDENT EEICT 2020 Selected Papers",
  year="2020",
  series="1",
  number="25",
  pages="103--107",
  isbn="978-80-214-5868-0"
}