Special techniques of instrumental analysis
FCH-DA_STIAk. rok: 2021/2022
Doporučená nebo povinná literatura
Christian G. D., O'Reilly J. E.: Instrumental Analysis. Allyn and Bacon, Boston 1986. (EN)
Způsob a kritéria hodnocení
Study results are verified pursuant to Article 34, Paragraph 7 of Study and Examination Rules of BUT. Students are given a credit for submitting protocols for each technique they studied. Protocols are processed in the following format: principles of the technique, the aim and exact methods used for measurement, collected data, their evaluation and interpretation, assessment of the impact of the technique on biophysical practice.
Fundamentals, instrumentation and usage of methods of chemical, physical and structure analysis. Separation methods: chromatography methods-gas chromatography, liquid chromatography, supercritical fluid chromatography; electrophoresis, isotachophoresis. Electroanalysis: special voltammetry. Atomic spectrometry: Atomic emission spectrometry, atomic absorption spectrometry, atomic fluorescence spectrometry. X-ray fluorescence spectrometry. Mass spectrometry organic and inorganic. Infrared and Raman spectroscopy. Nuclear magnetic resonance spectroscopy. Electron spin resonance spectroscopy. Moessbauer spectrometry. Hyphenated techniques. Viscosity and its measurement. Kinematics of stationary simple shear flow, dynamics of simple shear flow of viscous liquids, shear response of viscoelastic materials. Linear viscoelasticity, complex viscosity. Elongational viscosity. Rheology of polymers, suspensions and emulsions.