Course detail

Methods of Instrumental Analysis

FCH-MC_MIAAcad. year: 2021/2022

Instrumental techniques for characterization of properties of colloids (particles size and charge, interactions, thermodynamic and transport properties) and surface (wetting, contact angle, atomic force microscopy), methods for analysis of colloidal and special materials (thermic, viscoelastic, electric and electro-optical properties, microscopy).

Language of instruction

Czech

Number of ECTS credits

4

Mode of study

Not applicable.

Learning outcomes of the course unit

Students attending the course will be able to describe the basic principles of selected methods of structural analysis and methods for characterisation of colloidal systems and materials used in modern chemistry and chemical technology and for surface analysis. Student will be able to select appropriate method for given analysis, its basic settings and make data processing.

Prerequisites

physical chemistry, analytical chemistry

Co-requisites

Not applicable.

Planned learning activities and teaching methods

The course uses teaching methods in form of Lecture - 2 teaching hours per week. The e-learning system (LMS Moodle) is available for teachers and students.

Assesment methods and criteria linked to learning outcomes

Written and oral exam.

Course curriculum

Characterization of colloidal systems and surfaces
1. Size distribution of particles and macromolecules (light scattering, SEC)
2. Charge (zeta potential) and wetting of surface, contact angle
3. Atomic force microscopy (AFM)
4. Chemical and struktural analysis of dispersions
5. Transport properties (sorption and diffusion techniques
Materials analysis
6. Thermochemical analysis and microcalorimetry (DSC, TG, ITC)
7. Rheology and viscometry
8. Technology of thin layers preparation
9. Electric and electro-optical properties
10. Microscopy (optical and electron)

Work placements

Not applicable.

Aims

Describe the principles of selected techniques of structural analysis, methods used for characterisation of colloidal systems and materials generally used in modern chemistry, chemical technology and in surface analysis. Describe the ways how to select appropriate instrumental technique, settings the measurement parameters and data processing.

Specification of controlled education, way of implementation and compensation for absences

Attendance to lectures is not required but is recommended.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Skoog, D. A, Holler, J.: Principles of instrumental analysis, Cengage Learning, 2017. (EN)
Sommer, L.: Teoretické základy analytické chemie I, II, III, VUTIUM, 1995, 1998, 2000. (CS)
Klouda, P.: Moderní analytické metody, Ostrava: Nakladatelství Pavel Klouda, 1996.
Bartovská, L.; Šišková, M.: Fyzikální chemie povrchů a koloidních soustav, Praha: VŠCHT, 2005. (CS)

Recommended reading

Harris, D.C.: Exploring Chemican Analysis, W. H. Freeman, 2012. (EN)
Podzimek, Š.: Light Scattering, Size Exclusion Chromatography and AF4, Wiley, 2015. (EN)
Mezger, T.G.: Applied Rheology, Anton Paar, 2014. (EN)

eLearning

Classification of course in study plans

  • Programme NPCP_CHCHTE Master's, 1. year of study, winter semester, compulsory
  • Programme NKCP_CHCHTE Master's, 1. year of study, winter semester, compulsory

Type of course unit

 

Guided consultation in combined form of studies

26 hours, obligation not entered

Teacher / Lecturer

eLearning