Course detail

Analytical Chemistry II

FCH-BCA_ANC2Acad. year: 2012/2013

This course aims to introductuion students to the basic methods and techniques of instrumental analytical chemistry. Teaching is structured in the following thematic areas:Physical aspects of analytical methods. Analytical signal and its qulitative and quantitative evaluation. Principles of selected instrumental methods-spectrometric and electroanalytical methods, their qualitative and quantitative aspects and practical examples. Principles of selected separation methods, principles of chromatographic and electromigration methods. Evaluation of analytical results. Basics of chemometry. Preparation and decomposition of inorganic, organic and biological samples for analysis.

Language of instruction

Czech

Number of ECTS credits

6

Mode of study

Not applicable.

Learning outcomes of the course unit

By completion of the course the student will gain the following knowledge and skills:

1. They will know in depth the principles of simple instrumental analytical methods and possibilities of their application.
2. They will be able to select the optimal method for solving of specific analytical problems of analytical practice.
3. They will adopt the basic principles of chemometrictreatment of analytical results obtained using simple instrumental-analytical methods.

Prerequisites

Completion of the course Analytical chemistry I.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

Teaching methods depend on the type of course unit as specified in the article 7 of BUT Rules for Studies and Examinations.

Assesment methods and criteria linked to learning outcomes

Credit for the successful mastering written tests in computational exercises.
Condition for passing the exam is a credit from the exercise of Analytical Chemistry II.
The exam is oral, the degree of knowledge of the fundamentals of theory and practice of analytical chemistry and creative approach in solving analytical problems is assessed.

Course curriculum

Block 1: Electroanalytical methods
Potentiometry
Voltammetry, polarography (classic, differential pulse, dissolition, adsorptive)
Potentiometric dissolution analysis, titrations with polarizable electrodes¨
Electrogravimetry, coulometry, conductometry.

Block 2: Optical methods
Classification of spectral methods, basic physical principles, properties of electromagnetic radiation
Non-spectral methods: Refractometry, interferometry, polarimetry, nephelometry, turbidimetry
Spectral methods: UV-VIS spectrophotometry - principles, properties, construction of spectrophotometers, applications
Luminescence methods: molecular fluorescence, phosphorescence, chemiluminiscence, bioluminiscence and their analytical applications
Basics of otical atomic spectrometry

Block 3: Principles and applications of basic chromatographic and electromigration techniques
Basic principles of chromatography, separation mechanisms
Chromatographic techniques - paper chromtaography, thin-layer chromatography, column chromatography
Basics of modern liquid and gas chromatography
Separation in electric field - principles, application (electrophoresis)

Work placements

Not applicable.

Aims

The aim of the course is to provide students with an overview of selected instrumental analytical methods from the field of electrochemistry, spectrophotometry and separation techniques and to familiarize them with the strengths and limitations of these techniques. Students will also be introduced to chemometric approaches appropriate for processing the results obtained by these methods.

Specification of controlled education, way of implementation and compensation for absences

Written test in the course of semester.
Consultations for students in distant form.
Consultations for regular students.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Sommer L.: Základy analytické chemie II. VUTIUM, Brno 1998. (CS)
Volka K.: Analytická chemie II. VŠCHT Praha, 1997. (CS)
Kotouček M., Skopalová J.: Příklady z analytické chemie. Vydavatelství Univerzity Palackého Olomouc, 1997. (CS)

Recommended reading

Not applicable.

Classification of course in study plans

  • Programme BPCP_CHCHT_AKR Bachelor's

    branch BPCO_SCH , 2. year of study, summer semester, compulsory

  • Programme BKCP_CHCHT Bachelor's

    branch BKCO_SCH , 2. year of study, summer semester, compulsory

  • Programme BPCP_CHCHT Bachelor's

    branch BPCO_SCH , 2. year of study, summer semester, compulsory
    branch BPCO_CHTOZP , 2. year of study, summer semester, compulsory

  • Programme BPCP_CHCHT_AKR Bachelor's

    branch BPCO_CHTOZP , 2. year of study, summer semester, compulsory

  • Programme BKCP_CHCHT Bachelor's

    branch BKCO_CHTOZP , 2. year of study, summer semester, compulsory

  • Programme BPCP_CHCHT Bachelor's

    branch BPCO_CHTOZP , 2. year of study, summer semester, compulsory
    branch BPCO_CHMN , 2. year of study, summer semester, compulsory

  • Programme BKCP_CHCHT Bachelor's

    branch BKCO_CHM , 2. year of study, summer semester, compulsory

  • Programme BPCP_CHCHT_AKR Bachelor's

    branch BPCO_CHM , 2. year of study, summer semester, compulsory

  • Programme BPCP_CHCHT Bachelor's

    branch BPCO_CHM , 2. year of study, summer semester, compulsory

  • Programme BPCP_CHTP Bachelor's

    branch BPCO_BT , 2. year of study, summer semester, compulsory

  • Programme BKCP_CHTP Bachelor's

    branch BKCO_BT , 2. year of study, summer semester, compulsory
    branch BKCO_PCH , 2. year of study, summer semester, compulsory

  • Programme BPCP_CHTP Bachelor's

    branch BPCO_CHP , 2. year of study, summer semester, compulsory

  • Programme CKCP_CZV lifelong learning

    branch CKCO_CZV , 1. year of study, summer semester, compulsory

Type of course unit

 

Lecture

26 hours, optionally

Teacher / Lecturer

Guided consultation in combined form of studies

65 hours, optionally

Teacher / Lecturer

Exercise

26 hours, compulsory

Teacher / Lecturer