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Bachelor's Thesis
Author of thesis: Ing. Petr Lepcio, Ph.D.
Acad. year: 2011/2012
Supervisor: prof. RNDr. Vladimír Čech, Ph.D.
Reviewer: doc. Ing. Ota Salyk, CSc.
This bachelor thesis deals with preparation of thin films of plasma polymers prepared by plasma-enhanced chemical vapor deposition. Tetravinylsilane was used as a monomer. Two sets of samples were prepared. Samples of the first set were prepared at different effective powers from pure tetravinylsilane and samples of the second set were prepared from deposition mixture of tetravinylsilane with different oxygen content at constant effective power. The film thickness was evaluated by spectroscopic ellipsometry and chemical structure by infrared spectroscopy. A scratch test was used to determine adhesion characterized by the critical normal load. An appearance of performed scratches was obtained by atomic force microscopy (AFM). Film adhesion influenced by the effective power and oxygen content in deposition mixture was discussed based on the received data.
Plasma polymers, PECVD, tetravinylsilane, spectroscopic ellipsometry, adhesion, scratch test, atomic force microscopy (AFM)
Date of defence
19.06.2012
Result of the defence
Defended (thesis was successfully defended)
Grading
A
Process of defence
Výborně prezentovaná bakalářská práce. Diskuze se členy komise proběhla na velmi vysoké odborné úrovni studenta.
Language of thesis
Czech
Faculty
Fakulta chemická
Department
Institute of Materials Science
Study programme
Chemistry and Chemical Technologies (BPCP_CHCHT)
Field of study
Chemistry, Technology and Properties of Materials (BPCO_CHM)
Composition of Committee
prof. RNDr. Josef Jančář, CSc. (předseda) prof. Ing. Jaromír Havlica, DrSc. (místopředseda) prof. Ing. Ladislav Omelka, DrSc. (člen) doc. RNDr. Jaroslav Petrůj, CSc. (člen) prof. Ing. Tomáš Svěrák, CSc. (člen)
Supervisor’s reportprof. RNDr. Vladimír Čech, Ph.D.
Grade proposed by supervisor: A
Reviewer’s reportdoc. Ing. Ota Salyk, CSc.
Grade proposed by reviewer: A
Responsibility: Mgr. et Mgr. Hana Odstrčilová