Course detail
Modern Instrumental Methods for Material Analysis
FCH-DA_MIMAcad. year: 2022/2023
The detailed principles of the methods, the requirements for samples and their preprocessing, the typical outputs of measured data, the methods of data treatment and evaluation, the intepretation of the results, the analytical limits of the methods, the typical applications of the methods and the alternative methods.
X-ray diffraction analysis
X-ray fluorescence spectrometry
X-ray photo-electron spectrometry
NMR spectrometry
Raman spectrometry/microscopy
IR spectrometry
Scanning and transmission electron microscopy
Microscopy of atomic forces
Thermal analysis - TGA-DTA(DSC)-EGA-TMA
Optical emission spectrometry in inductive coupled plasma
Ion chromatography
Guarantor
Department
Learning outcomes of the course unit
X-ray diffraction analysis
X-ray fluorescence spectrometry
X-ray photo-electron spectrometry
NMR spectrometry
Raman spectrometry/microscopy
IR spectrometry
Scanning and transmission electron microscopy
Knowledge of priciples of methods, processing and interpretation of results, analytical limits and typical applications of these metods:
Microscopy of atomic forces
Thermal analysis - TGA-DTA(DSC)-EGA-TMA
Optical emission spectrometry in inductive coupled plasma
Ion chromatography
Prerequisites
Basic knowledge of general and inorganic chemistry, physical chemistry and materials physics and analytical chemistry.
Co-requisites
Not applicable.
Recommended optional programme components
Not applicable.
Recommended or required reading
Not applicable.
Planned learning activities and teaching methods
The teaching is realized mainly via individual consultations. In the case of the selected instrumental analytical methods the teaching is also carried directly at the instrument with assistance of the operator of instrument.
Assesment methods and criteria linked to learning outcomes
The gained knowledge will be verified via oral examination and via prepared project of measured and evaluated data at the selected analytical equipment.
Language of instruction
English
Work placements
Not applicable.
Course curriculum
The detailed principles of the methods, the requirements for samples and their preprocessing, the typical outputs of measured data, the methods of data treatment and evaluation, the intepretation of the results, the analytical limits of the methods, the typical applications of the methods and the alternative methods.
X-ray diffraction analysis
X-ray fluorescence spectrometry
X-ray photo-electron spectrometry
NMR spectrometry
Raman spectrometry/microscopy
IR spectrometry
Scanning and transmission electron microscopy
Microscopy of atomic forces
Thermal analysis - TGA-DTA(DSC)-EGA-TMA
Optical emission spectrometry in inductive coupled plasma
Ion chromatography
Aims
The of the course is to get deeper knowledge and skills in the field of selected advanced instumental methods of chemical, phase, structure and thermal analysis. Student gets to know the principals, measurement routes and experimental data treatment and evaluation. After a consultation with superviser the student also receives practical training at selected equipments led by the operator.
Specification of controlled education, way of implementation and compensation for absences
Teaching is not checked during the semester.
Classification of course in study plans
- Programme DKAP_CHM_4_N Doctoral, 1. year of study, winter semester, 0 credits, compulsory-optional
- Programme DPAP_CHM_4_N Doctoral, 1. year of study, winter semester, 0 credits, compulsory-optional