Course detail
Materialography
FSI-WMGAcad. year: 2010/2011
Basic methods of examining the structure of metallic and ceramic materials. Preparation of metallographic specimens for various methods of structure imaging, qualitative and quantitative structure evaluation aimed at finding the relations that exist between the structure and the mechanical and physical properties of materials.
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Course curriculum
2. Metallographic sampling for metallographic analysis. Selection of a metallographic sample position. Metallographic cut sample orientation, metallographic sample surface. Technological aspects of suitability of the sample selection. Influence of the sampling method on the structure.
3. Grinding, polishing of samples for light microscopy observation. Mechanical polishing, electrolytic polishing, chemical polishing. Laboratory techniques of semi-automatic and automatic preparation of metallographic samples. Etching, colour etching.
4. Structure observation of non-etching samples. Steel purity determination. Baumann printing. Etching samples observation (selection). Macroscopic etching and observation.
5. Replicas preparation. Foils preparation. Samples for scanning electron microscopy.
6. The most frequent types of steels selection and cast iron their structure valuation in terms of standards ČSN.
7. Individual work. Sample preparation and evaluation of the structure (method selection) of the given ferroalloy material.
8. Specific features of copper alloy samples preparation (Cu, Bronze cast and wrought, Brass cast and wrought)
9. Aluminium alloy (cast, wrought, hardenable and non-hardenable) sample preparation.
10. Study of corrosion (outlines). Study of cavitations. Possibilities of studying fatigue processes. Liquation, segregation and study of other non-homogeneities.
11. Bimetal and sandwich composites metallography. Basic aspects of ceramic-metallic materials, SAPs and sintered carbides preparation.
12. Systemization and classification of fractures. Fracture area evaluation methods.
13. Methods of the quantitative evaluation of the structure. Spatial arrangement of structure components (stereo-logical models).
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Syllabus
2. Preparation procedure of metallographic samples.
3. Light microscopy.
4. Samples preparation for electron microscopy.
5. Steel and cast iron metallography.
6. Nonferrous metals, copper alloys.
7. Nonferrous metals, aluminium alloys.
8. Nonferrous metals, metallography of zinc alloys, metallography of heavy metals (composition).
9. Metallographic methods of studying selected degradation processes.
10. Metal complexes metallography.
11. Composite materials metallography.
12. Fractography.
13. Stereoscopic and stereometric metallography.