Microstructure and mechanical properties of Ni1,5Co1,5CrFeTi0,5 high entropy alloy fabricated by mechanical alloying and spark plasma sintering

Microstructure and mechanical properties of Ni1,5Co1,5CrFeTi0,5 high entropy alloy fabricated by mechanical alloying and spark plasma sintering

WoS Article

The present work is focused on synthesis and mechanical properties evaluation of non-equiatomic Ni1,5Co1,5CrFeTi0,5, ductile single phase high entropy alloy (HEA) with excellent mechanical properties (bend strength Rmb = 2593 MPa, tensile strength Rm = 1384 MPa, tensile elongation to fracture of 4.01%, and elastic modulus of 216 GPa) surpassing those of traditional as-cast HEA. For the alloy production, a combination of mechanical alloying (MA) process in a planetary ball mill and spark plasma sintering (SPS) for powder densification was utilized. The tensile properties of a bulk material produced by a combination of MA+SPS are characterized for the first time. The feedstock powder and corresponding bulk material microstructure, elemental and phase composition, and mechanical properties were investigated by scanning (SEM) and transmission (TEM) electron microscopy, energy-dispersive X-ray spectroscopy (EDX), electron backscatter diffraction (EBSD), X-ray diffraction (XRD), aswell as impulse excitation of vibration, Vickers microhardness and tensile and bend strength tests, respectively. The structure of the samples consisted of single-phase FCC high entropy solid solution of extremely fine-twinned grains and oxide inclusions inherited from the original powder feedstock. Dimple-like morphology corresponding to ductile fracture mode has been observed on the fracture surfaces, with crack initiation sites on the inclusions phases.

The present work is focused on synthesis and mechanical properties evaluation of non-equiatomic Ni1,5Co1,5CrFeTi0,5, ductile single phase high entropy alloy (HEA) with excellent mechanical properties (bend strength Rmb = 2593 MPa, tensile strength Rm = 1384 MPa, tensile elongation to fracture of 4.01%, and elastic modulus of 216 GPa) surpassing those of traditional as-cast HEA. For the alloy production, a combination of mechanical alloying (MA) process in a planetary ball mill and spark plasma sintering (SPS) for powder densification was utilized. The tensile properties of a bulk material produced by a combination of MA+SPS are characterized for the first time. The feedstock powder and corresponding bulk material microstructure, elemental and phase composition, and mechanical properties were investigated by scanning (SEM) and transmission (TEM) electron microscopy, energy-dispersive X-ray spectroscopy (EDX), electron backscatter diffraction (EBSD), X-ray diffraction (XRD), aswell as impulse excitation of vibration, Vickers microhardness and tensile and bend strength tests, respectively. The structure of the samples consisted of single-phase FCC high entropy solid solution of extremely fine-twinned grains and oxide inclusions inherited from the original powder feedstock. Dimple-like morphology corresponding to ductile fracture mode has been observed on the fracture surfaces, with crack initiation sites on the inclusions phases.

Multi principal element alloy Tensile strength Fracture Ductility

Multi principal element alloy Tensile strength Fracture Ductility

MORAVČÍK, I.; ČÍŽEK, J.; ZAPLETAL, J.; KOVACOVA, Z.; VESELY, J.; MINÁRIK, P.; KITZMANTECH, M.; NEUBAUER, E.; DLOUHÝ, I.

2018

16.01.2017

ELSEVIER SCI LTD, THE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD OX5 1GB, OXON, ENGLAND

OXON, ENGLAND

1873-4197

MATERIALS & DESIGN

119

1

United Kingdom of Great Britain and Northern Ireland

141

151

10

http://www.sciencedirect.com/science/article/pii/S0264127517300461

http://hdl.handle.net/

1-s2.0-S0264127517300461-main