Publication result detail

Dilatometric and microstructural study of particle and functionally graded composites based on hydroxyapatite and crystalline bioglass

DRDLÍK, D.; DRDLÍKOVÁ, K.; MACA, K.

Original Title

Dilatometric and microstructural study of particle and functionally graded composites based on hydroxyapatite and crystalline bioglass

English Title

Dilatometric and microstructural study of particle and functionally graded composites based on hydroxyapatite and crystalline bioglass

Type

WoS Article

Original Abstract

Hydroxyapatite (HA) and bioglass (BG) ceramics have become of prime importance in bone tissue engineering. Besides the appropriate composition, the microstructure of bone replacement plays a crucial role. In the present work, particle composites and functionally graded material (FGM) based on HA and BG prepared by electrophoretic deposition were thoroughly characterised in terms of the preparation method, sintering process, phase composition and microstructure. The sintering was monitored by high-temperature dilatometry in two directions, the sintering rates were calculated, and the overall sintering process was discussed. The SEM showed the continuous change in the microstructure of FGM with gradual interconnected porosity favourable for bio-applications. The fundamental fractographic analysis proved the crack development in FGM related to the sintering process, and the recommendations for the reduction of the crack development were given. The phase transformations during thermal treatment were analysed using X-ray diffraction analysis and deeply discussed.

English abstract

Hydroxyapatite (HA) and bioglass (BG) ceramics have become of prime importance in bone tissue engineering. Besides the appropriate composition, the microstructure of bone replacement plays a crucial role. In the present work, particle composites and functionally graded material (FGM) based on HA and BG prepared by electrophoretic deposition were thoroughly characterised in terms of the preparation method, sintering process, phase composition and microstructure. The sintering was monitored by high-temperature dilatometry in two directions, the sintering rates were calculated, and the overall sintering process was discussed. The SEM showed the continuous change in the microstructure of FGM with gradual interconnected porosity favourable for bio-applications. The fundamental fractographic analysis proved the crack development in FGM related to the sintering process, and the recommendations for the reduction of the crack development were given. The phase transformations during thermal treatment were analysed using X-ray diffraction analysis and deeply discussed.

Keywords

Bioglass; Functionally graded material; Hydroxyapatite; Microstructure; Sintering

Key words in English

Bioglass; Functionally graded material; Hydroxyapatite; Microstructure; Sintering

Authors

DRDLÍK, D.; DRDLÍKOVÁ, K.; MACA, K.

RIV year

2024

Released

23.10.2023

ISBN

0350-820X

Periodical

SCIENCE OF SINTERING

Volume

55

Number

3

State

Republic of Serbia

Pages from

289

Pages to

306

Pages count

18

URL

http://ojs.itn.sanu.ac.rs/index.php/scisint/article/view/1099

Full text in the Digital Library

http://hdl.handle.net/11012/245085

BibTex

@article{BUT184960,
  author="Daniel {Drdlík} and Katarina {Drdlíková} and Karel {Maca}",
  title="Dilatometric and microstructural study of particle and functionally graded composites based on hydroxyapatite and crystalline bioglass",
  journal="SCIENCE OF SINTERING",
  year="2023",
  volume="55",
  number="3",
  pages="289--306",
  doi="10.2298/SOS221028017D",
  issn="0350-820X",
  url="http://ojs.itn.sanu.ac.rs/index.php/scisint/article/view/1099"
}

Documents

0350-820X2300017D