Publication result detail

Preparation of magnetic nanoparticles by one step synthesis with morphology of particles changed based on time of reaction and temperature treatment

SOLNÝ, T.; DLABAJOVÁ, L.; OPRAVIL, T.; PTÁČEK, P.; BŘEZINA, M.; ŠVEC, J.; MÁSILKO, J.; AMBAT, R.

Original Title

Preparation of magnetic nanoparticles by one step synthesis with morphology of particles changed based on time of reaction and temperature treatment

English Title

Preparation of magnetic nanoparticles by one step synthesis with morphology of particles changed based on time of reaction and temperature treatment

Type

WoS Article

Original Abstract

In present study, nanosized iron oxides particles are synthetised by easy one step precipitation from Mohric salt (NH4)(2)Fe(SO4)(2)center dot 6H(2)O reacting with sodium hydroxide solution in temperature up to 60 degrees C. When changing the time of reaction, the iron oxide particles of different shape are prepared and when drying wet extracted particles at elevated temperature of 60 degrees C the change of 2D shaped morphology is observed. Depending on the time of reaction different ratios of FeOOH and Fe3O4 are obtained in this study. DTA - TGA, XRD, FTIR and SEM are used for the characterisation of particles in this study.

English abstract

In present study, nanosized iron oxides particles are synthetised by easy one step precipitation from Mohric salt (NH4)(2)Fe(SO4)(2)center dot 6H(2)O reacting with sodium hydroxide solution in temperature up to 60 degrees C. When changing the time of reaction, the iron oxide particles of different shape are prepared and when drying wet extracted particles at elevated temperature of 60 degrees C the change of 2D shaped morphology is observed. Depending on the time of reaction different ratios of FeOOH and Fe3O4 are obtained in this study. DTA - TGA, XRD, FTIR and SEM are used for the characterisation of particles in this study.

Keywords

Magnetic nanoparticles; FeOOH; iron oxides

Key words in English

Magnetic nanoparticles; FeOOH; iron oxides

Authors

SOLNÝ, T.; DLABAJOVÁ, L.; OPRAVIL, T.; PTÁČEK, P.; BŘEZINA, M.; ŠVEC, J.; MÁSILKO, J.; AMBAT, R.

RIV year

2021

Released

01.01.2021

Publisher

Taylor & Francis

Location

ABINGDON

ISBN

1745-8099

Periodical

Journal of Experimental Nanoscience

Volume

16

Number

1

State

United Kingdom of Great Britain and Northern Ireland

Pages from

1

Pages to

10

Pages count

10

URL

https://www.tandfonline.com/doi/full/10.1080/17458080.2020.1844880

Full text in the Digital Library

http://hdl.handle.net/11012/196357

BibTex

@article{BUT169558,
  author="SOLNÝ, T. and DLABAJOVÁ, L. and OPRAVIL, T. and PTÁČEK, P. and BŘEZINA, M. and ŠVEC, J. and MÁSILKO, J. and AMBAT, R.",
  title="Preparation of magnetic nanoparticles by one step synthesis with morphology of particles changed based on time of reaction and temperature treatment",
  journal="Journal of Experimental Nanoscience",
  year="2021",
  volume="16",
  number="1",
  pages="1--10",
  doi="10.1080/17458080.2020.1844880",
  issn="1745-8080",
  url="https://www.tandfonline.com/doi/full/10.1080/17458080.2020.1844880"
}

Documents

1844880