Publication result detail

Optimization of the HS-SPME method coupled with GC/uECD for determination of methylmercury in water

KRÁLOVÁ, Z.; VÁVROVÁ, M.; ŠUCMAN, E.; KOMÁRKOVÁ, P.

Original Title

Optimization of the HS-SPME method coupled with GC/uECD for determination of methylmercury in water

English Title

Optimization of the HS-SPME method coupled with GC/uECD for determination of methylmercury in water

Type

WoS Article

Original Abstract

The aim of this study was the optimization of the Solid Phase Micro-extraction (SPME) method and the optimization of gas chromatography using an electron capture detector method. The analytical procedure involves derivatization of ionic mercury with sodium tetraethylborate in a sample vial and following extraction with a silica polydimethylsiloxane coated fibre.

English abstract

The aim of this study was the optimization of the Solid Phase Micro-extraction (SPME) method and the optimization of gas chromatography using an electron capture detector method. The analytical procedure involves derivatization of ionic mercury with sodium tetraethylborate in a sample vial and following extraction with a silica polydimethylsiloxane coated fibre.

Keywords

methylmercury, solid phase micro-extraction, optimization, gas chromatography

Key words in English

methylmercury, solid phase micro-extraction, optimization, gas chromatography

Authors

KRÁLOVÁ, Z.; VÁVROVÁ, M.; ŠUCMAN, E.; KOMÁRKOVÁ, P.

RIV year

2015

Released

15.12.2014

ISBN

1018-4619

Periodical

Fresenius Environmental Bulletin

Volume

23

Number

12B

State

Federal Republic of Germany

Pages from

3362

Pages to

3365

Pages count

4

BibTex

@article{BUT111051,
  author="Zuzana {Králová} and Milada {Vávrová} and Emanuel {Šucman} and Petra {Komárková}",
  title="Optimization of the HS-SPME method coupled with GC/uECD for determination of methylmercury in water",
  journal="Fresenius Environmental Bulletin",
  year="2014",
  volume="23",
  number="12B",
  pages="3362--3365",
  issn="1018-4619"
}